E – 02 Standard Test Methods for Determination of Carbon, Sulfur, Nitrogen, and Oxygen in Steel and in Iron, Nickel, and Cobalt Alloys, cobalt alloys. ASTM E Standard Test Methods for Determination of Carbon, Sulfur, Nitrogen, and Oxygen in Steel, Iron, Nickel, and Cobalt Alloys by. ASTM E Standard Test Methods for Determination of Carbon, Sulfur, Nitrogen, and Oxygen in Steel, Iron, Nickel, and Cobalt Alloys by Various Combustion.
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Make a minimum of two determinations using a specimen as directed in Metal analysis Since D-lab is accredited for analyses of steel. If necessary, wash three times with acetone by decantation to remove organic contaminants and dry at room temperature.
The energy of this wavelength is absorbed as the gas passes through a cell body in which the IR energy is transmitted. Cool in a desiccator. However, recognizing that commercial oxygen determinators zstm capable of handling higher concentrations, it may be that this test method can be used for oxygen concentrations outside of the scope. As written, this test method is not applicable to cast iron samples. Add to Alert PDF. We have no amendments or corrections for this standard.
Make the required power, gas, and water connections. Additional elements not included in the table will cause extra cost.
During specimen combustion, the ow of CO2 with its oxygen gas carrier is routed through the measure chamber while oxygen alone passes through the reference chamber.
The scopes are reviewed annually by Swedac. Blank values are equal to the total result of the accelerator and Calibrant A minus the certied value for the calibrant. Need more than one copy? During specimen combustion, the ow of SO2 with its oxygen gas carrier is routed through the measure chamber while oxygen alone passes through the reference chamber. We have no document history for this standard. Crucibles may be placed in a desiccator for periods of 1 h prior to use.
NOTE 8—Repeat the calibration when: NOTE 33—Although these test methods were tested to only 0. Since the output of most modern instruments is given directly in percent concentration, post-analysis calculations may not be required. This creates an IR energy imbalance reaching the diaphragm and thus distorting it. Treat each capsule as directed in Use Calibrant CCC as the certied reference material and analyze at least three specimens to determine the calibration slope.
Specific hazards statements are given in Section 6. Please first verify your email before subscribing to alerts. NOTE 1—The accelerator should contain no more than 0. You can download and open this file to your own computer but DRM prevents opening this file on another computer, including a networked server.
NOTE 27—The uncertainty of results obtained using this test method is dependent on the uncertainty of the values assigned to the calibration reference materials. Atsm a minimum of e0119 determinations using the specimen and accelerator as directed in No other units of measurement are included in this standard. It is expected that work will be performed in a properly equipped laboratory.
As the voice of the U. Originally approved in Nitrogen present in the sample is released as molecular nitrogen into the owing 6 Supporting data are available from ASTM International Headquarters. If they are not analyzed within four hours of preparation, repeat the ling step or grinding step prior to analysis. Test the furnace and the analyzer to ensure the absence of leaks.
The water is then absorbed by magnesium perchlorate and the remaining nitrogen and carbon dioxide are separated chromatographically. The analyses are made for a limited number of elements per alloy. The results should be within the allowable limits of the certied reference material. Subscription pricing is determined by: Note 22—The upper limit of the scope has been set at 0.
In this case, laboratories should perform method validation using reference materials. Standards Subsctiption may be the perfect solution.
It is the responsibility astmm the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Precision and Bias In the absence of CO and CO2, the energy received by each detector is maximum. During combustion, the IR absorption properties of the SO 2 gas in the chamber causes a loss of energy, therefore a loss in signal results which is proportional to the concentration of the gas in the closed loop.